Monomer-on-Monomer (MoM) Mitsunobu Reaction: Facile Purification Utilizing Surface-Initiated Sequestration

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Issue Date
2011-01-07Author
Maity, Pradip K.
Rolfe, Alan
Samarakoon, Thiwanka Bandara
Faisal, Saqib
Kurtz, Ryan D.
Long, Toby R.
Schätz, Alexander
Flynn, Daniel L.
Grass, Robert N.
Stark, Wendelin J.
Reiser, Oliver
Hanson, Paul R.
Publisher
American Chemical Society
Type
Article
Article Version
Scholarly/refereed, author accepted manuscript
Rights
This document is the Accepted Manuscript version of a Published Work that appeared in final form in Organic Letters, copyright © American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see http://dx.doi.org/10.1021/ol1022382.
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Show full item recordAbstract
A monomer-on-monomer (MoM) Mitsunobu reaction utilizing norbornenyl-tagged (Nb-tagged) reagents is reported, whereby purification was rapidly achieved by employing ring-opening metathesis polymerization which is initiated by any of three methods utilizing Grubbs catalyst (i) free catalyst in solution, (ii) surface-initiated catalyst-armed silica or (iii) surface-initiated catalyst-armed Co/C magnetic nanoparticles.
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Citation
Maity, P. K., Rolfe, A., Samarakoon, T. B., Faisal, S., Kurtz, R. D., Long, T. R., … Hanson, P. R. (2011). Monomer-on-Monomer (MoM) Mitsunobu Reaction: Facile Purification Utilizing Surface-Initiated Sequestration. Organic Letters, 13(1), 8–10. http://doi.org/10.1021/ol1022382
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