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Intramolecular monomer-on-monomer (MoM) mitsunobu cyclization for the synthesis of benzofused thiadiazepine-dioxides
Maity, Pradip K. Kainz, Quirin M. Faisal, Saqib Rolfe, Alan Samarakoon, Thiwanka Bandara Basha, Fatima Z. Reiser, Oliver Hanson, Paul R.
Maity, Pradip K.
Kainz, Quirin M.
Faisal, Saqib
Rolfe, Alan
Samarakoon, Thiwanka Bandara
Basha, Fatima Z.
Reiser, Oliver
Hanson, Paul R.
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Abstract
The utilization of a monomer-on-monomer (MoM) intramolecular Mitsunobu cyclization reaction employing norbornenyl-tagged (Nb-tagged) reagents is reported for the synthesis of benzofused thiadiazepine-dioxides. Facile purification was achieved via ring-opening metathesis (ROM) polymerization initiated by one of three metathesis catalyst methods: (i) free metathesis catalyst, (ii) surface-initiated catalyst-armed silica, or (iii) surface-initiated catalyst-armed Co/C magnetic nanoparticles.
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2012-06-14
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Royal Society of Chemistry
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Maity, Pradip K., Quirin M. Kainz, Saqib Faisal, Alan Rolfe, Thiwanka. B. Samarakoon, Fatima Z. Basha, Oliver Reiser, and Paul R. Hanson. "Intramolecular Monomer-on-monomer (MoM) Mitsunobu Cyclization for the Synthesis of Benzofused Thiadiazepine-dioxides." Chemical Communications 47.46 (2011): 12524.