Xu, ChangqiZhang, ZhichengYe, QiangLiu, Xiong2016-08-032016-08-032003-01-28Xu, C., Zhang, Z., Ye, Q., & Liu, X. (2003, January 29). Synthesis of Copper Sulfide Nanowhisker via Sonochemical Way and its Characterization. Chemistry Letters, 32(2). doi:10.1246/cl.2003.198https://hdl.handle.net/1808/21255An ultrasonic irradiation route (USI route) is developed to synthesize whisker-like copper sulfide (Cu9S8) nanocrystals via the reaction between copper sulfate pantahydrate (CuSO4·5H2O) and thioacetamide (CH3CSNH2) in an aqueous solution at room temperature under ambient pressure. XRD, TEM, UV–vis and PL spectra are used to characterize the obtained product. A possible reaction process is suggested in the end of this paper.Copyright © 2003 The Chemical Society of JapanArticle10.1246/cl.2003.198openAccess