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Monomer-on-Monomer (MoM) Mitsunobu Reaction: Facile Purification Utilizing Surface-Initiated Sequestration
Maity, Pradip K. Rolfe, Alan Samarakoon, Thiwanka Bandara Faisal, Saqib Kurtz, Ryan D. Long, Toby R. Schätz, Alexander Flynn, Daniel L. Grass, Robert N. Stark, Wendelin J.
Maity, Pradip K.
Rolfe, Alan
Samarakoon, Thiwanka Bandara
Faisal, Saqib
Kurtz, Ryan D.
Long, Toby R.
Schätz, Alexander
Flynn, Daniel L.
Grass, Robert N.
Stark, Wendelin J.
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Abstract
A monomer-on-monomer (MoM) Mitsunobu reaction utilizing norbornenyl-tagged (Nb-tagged) reagents is reported, whereby purification was rapidly achieved by employing ring-opening metathesis polymerization which is initiated by any of three methods utilizing Grubbs catalyst (i) free catalyst in solution, (ii) surface-initiated catalyst-armed silica or (iii) surface-initiated catalyst-armed Co/C magnetic nanoparticles.
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2011-01-07
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American Chemical Society
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Maity_2011.pdf
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Maity, P. K., Rolfe, A., Samarakoon, T. B., Faisal, S., Kurtz, R. D., Long, T. R., … Hanson, P. R. (2011). Monomer-on-Monomer (MoM) Mitsunobu Reaction: Facile Purification Utilizing Surface-Initiated Sequestration. Organic Letters, 13(1), 8–10. http://doi.org/10.1021/ol1022382