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Oxidative Cyclization of Sulfamates onto Pendant Alkenes
Shinde, Anand H. Sathyamoorthi, Shyam
Shinde, Anand H.
Sathyamoorthi, Shyam
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Abstract
This communication discloses the first examples of aza-Wacker cyclizations of sulfamate esters. Within the realm of related cyclization reactions, this protocol is differential in that it forms six-membered rings in good yield and uses catalytic amounts of palladium(0) rather than palladium(II) salts. These reactions scale well, and their products are demonstrated to be valuable synthetic intermediates.
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This document is the Accepted Manuscript version of a Published Work that appeared in final form in Organic Letters, copyright © 2020 American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see https://doi.org/10.1021/acs.orglett.9b04448.
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2020-01-13
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American Chemical Society
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Shinde, A. H., & Sathyamoorthi, S. (2020). Oxidative Cyclization of Sulfamates onto Pendant Alkenes. Organic letters, 22(3), 896–901. https://doi.org/10.1021/acs.orglett.9b04448